Formamide, N-[(4-methoxyphenyl)methyl]-

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CAS: 17061-63-1
MF: C9H11NO2
MW: 165.18914
Synonyms: Formamide, N-[(4-methoxyphenyl)methyl]-

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Buxing Han

Institute of Chemistry, Chinese Academy of Sciences
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Feng Wang

Institute of Chemistry
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HuiZhen Liu

Institute of Chemistry
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Naoki Asao

Tohoku University
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Tom D. Sheppard

University College London
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Jonathan M. J. Williams

Department of Chemistry University of Bath Claverton Down
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Co-reporter: Ourida Saidi, Mark J. Bamford, A. John Blacker, James Lynch, Stephen P. Marsden, Pawel Plucinski, Robert J. Watson, Jonathan M.J. Williams
pp: 5804-5806
Publication Date(Web):3 November 2010
DOI: 10.1016/j.tetlet.2010.08.106
Amines have been formylated using aqueous formaldehyde or paraformaldehyde and the iridium catalyst [Cp∗IrI2]2. Paraformaldehyde acts as both a formylating agent and an oxidant.The reaction of amines with either formaldehyde or paraformaldehyde in water in the presence of [Cp∗IrI2]2 affords the corresponding formamides in good yields.Image for unlabelled figure

Rei Kinjo

Nanyang Technological University
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Jian Zhang

Chinese Academy of Sciences
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Shu Kobayashi

The University of Tokyo
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Feng Wang

Dalian Institute of Chemical Physics
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