Collect

BASIC PARAMETERS Find an error

CAS: 708251-87-0
MF: C16H12NO3Br
MW: 346.17538
Synonyms:

REPORT BY

Haifeng Du

Institute of Chemistry, Chinese Academy of Sciences
follow

Annaliese K. Franz

University of California
follow
Co-reporter: Joseph J. Badillo, Abel Silva-García, Benjamin H. Shupe, James C. Fettinger, Annaliese K. Franz
pp: 5550-5553
Publication Date(Web):26 October 2011
DOI: 10.1016/j.tetlet.2011.08.071
The condensation cyclization between isatins and 5-methoxy tryptamine catalyzed by chiral phosphoric acids provides spirooxindole tetrahydro-β-carboline products in excellent yields (up to 99%) and enantioselectivity (up to 98:2 er). A comparison of catalysts provides insight for the substrate scope and factors responsible for efficient catalytic activity and selectivity in the spirocyclization. Chiral phosphoric acids with different 3,3′-substitution on the binaphthyl system and opposite axial chirality afford the spiroindolone product with the same absolute configuration.Image for unlabelled figure